Kugelrohr Distillation

Kugelrohr Distillation. The solvent was removed under reduced pressure The residue was distilled under reduced pressure with a Kugelrohr distillation apparatus (190°C/09 mmHg) to give 11ditertbutyl12dichloro22diphenyldisilane (771 g 97%) as a colorless liquid This liquid solidified on standing at room temperature in 1 day.

Kugelrohr A Kugelrohr (literally “ball tube”) is a short path vacuum distillation apparatus typically used to distill relatively small amounts of high boiling (> 300 °C) compounds under greatly reduced pressure in the laboratory Additional recommended knowledge.

Kugelrohr distillation De Química

Shortpath distillation is a distillation technique that involves the distillate traveling a short distance often only a few centimeters and is normally done at reduced pressure Shortpath distillation systems often have a variety of names depending on the manufacturer of the system and what compounds are being distilled within them A classic example would be a distillation.

Kugelrohr at Thomas Scientific

Ordering a Kugelrohr Evaporator System $430422 – $453723 Includes distillation oven stirring module and stand Choose the sizes of the receiving bulb and distillation flask The bulb and flask joint size must match the joint size of the stirring module If you are unsure about which sizes to pick please contact us.

TechThursday XIX: Kugelrohr distillation YouTube

Kugelrohr shortpath distillation apparatus AC/DC input 230 V AC All Photos (5) Description General description Distills the most difficult materials! Distills heatsensitive compounds Distills liquids and lowmelting solids from polymers and tars Removes color and particulates Distills with minimal holdup and sample loss Can be used for sublimation/solvent evaporation Step.